2-phenyl-3,3-dimethylbutanamine

Base Information

Chemical Name:2-phenyl-3,3-dimethylbutanamine
CAS No.:27561-40-6
Molecular Formula:C₁₂H₁₉N
Molecular Weight:177.29
Hs Code.:

Synonyms:2-phenyl-3,3-dimethylbutanamine

Suppliers and Price of 2-phenyl-3,3-dimethylbutanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyl-3,3-dimethylbutanamine

Chemical Property:

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Technology Process of 2-phenyl-3,3-dimethylbutanamine

There total 9 articles about 2-phenyl-3,3-dimethylbutanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100366-87-8
α-(tert-butyl)phenylacetamide

: 27561-40-6
2-phenyl-3,3-dimethylbutanamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 20h; Yield given;
DOI:10.1021/jo00358a034

Reference yield:

: 938-16-9
2,2-dimethylpropiophenone

: 27561-40-6
2-phenyl-3,3-dimethylbutanamine

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / NaBH₄ / ethanol; methanol / 2 h

2: 72 percent / SOCl₂ / 23 °C

3: 1.) Mg, methyl iodide / 1.) THF, ether, reflux, 1 h, 2.) 0 deg C, 1 h

4: SOCl₂ / 1.5 h / Heating

5: 82 percent / concd. NH₄OH / diethyl ether / 0 °C

6: LiAlH₄ / diethyl ether / 20 h

With ammonium hydroxide; sodium tetrahydroborate; lithium aluminium tetrahydride; thionyl chloride; magnesium; methyl iodide; In methanol; diethyl ether; ethanol;
DOI:10.1021/jo00358a034

Reference yield:

: 1007-26-7
(2,2-dimethyl-1-propyl)benzene

: 27561-40-6
2-phenyl-3,3-dimethylbutanamine

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / SOCl₂ / 23 °C

2: 1.) Mg, methyl iodide / 1.) THF, ether, reflux, 1 h, 2.) 0 deg C, 1 h

3: SOCl₂ / 1.5 h / Heating

4: 82 percent / concd. NH₄OH / diethyl ether / 0 °C

5: LiAlH₄ / diethyl ether / 20 h

With ammonium hydroxide; lithium aluminium tetrahydride; thionyl chloride; magnesium; methyl iodide; In diethyl ether;
DOI:10.1021/jo00358a034