C₂₅H₂₉F₆N₃O₂

Base Information

Chemical Name:C₂₅H₂₉F₆N₃O₂
CAS No.:1563182-39-7
Molecular Formula:C₂₅H₂₉F₆N₃O₂
Molecular Weight:517.515
Hs Code.:

C<sub>25</sub>H<sub>29</sub>F<sub>6</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₂₅H₂₉F₆N₃O₂

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Chemical Property of C₂₅H₂₉F₆N₃O₂

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Technology Process of C₂₅H₂₉F₆N₃O₂

There total 4 articles about C₂₅H₂₉F₆N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2448-45-5
Cbz-D-Phe

: 1563182-39-7
C₂₅H₂₉F₆N₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: (1S)-10-camphorsulfonic acid / toluene / 0.5 h / Reflux; Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 18 h / 20 °C / Inert atmosphere

3.1: hydrogen; 10% palladium hydroxide on charcoal / methanol / 16 h / 20 °C / 760.05 Torr / Inert atmosphere

4.1: dichloromethane / 18 h / 20 °C / Inert atmosphere

4.2: 20 h / 20 °C / Inert atmosphere

5.1: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride / 1,4-dioxane / 48 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; 10% palladium hydroxide on charcoal; (1S)-10-camphorsulfonic acid; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In 1,4-dioxane; methanol; dichloromethane; toluene;
DOI:10.1021/ml400528y

Reference yield:

: C₃₀H₃₇F₆N₃O₄

: 1563182-39-7
C₂₅H₂₉F₆N₃O₂

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ml400528y

Reference yield:

: C₂₂H₂₁F₆NO₃

: 1563182-39-7
C₂₅H₂₉F₆N₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 48 h / 20 °C / Inert atmosphere

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In 1,4-dioxane; dichloromethane;
DOI:10.1021/ml400528y