bisyl(mesityl)dimethoxygermane

Base Information

Chemical Name:bisyl(mesityl)dimethoxygermane
CAS No.:136094-87-6
Molecular Formula:C₁₈H₃₆GeO₂Si₂
Molecular Weight:413.244
Hs Code.:

Synonyms:bisyl(mesityl)dimethoxygermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bisyl(mesityl)dimethoxygermane

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Technology Process of bisyl(mesityl)dimethoxygermane

There total 1 articles about bisyl(mesityl)dimethoxygermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 126529-82-6
tris(methoxy)mesitylgermane

: 41823-71-6
bis(trimethylsilyl)methyllithium

: 136094-87-6
bisyl(mesityl)dimethoxygermane

Guidance literature:: In diethyl ether; pentane; byproducts: MeOLi; under inert gas, bisylLi in Et2O added to Ge-compound in pentane at -78°C, warmed to room temp., refluxed for 4 h; filtered, evaporated in vacuo, recrystd. (pentane); elem. anal.;
DOI:10.1016/S0277-5387(00)86091-X

Reference yield: 76.0%

: 136094-87-6
bisyl(mesityl)dimethoxygermane

: 136094-88-7
bisyl(mesityl)difluorogermane

Guidance literature:: With hydrogen fluoride; In benzene; byproducts: MeOH; under inert gas, 40% aq. HF added to Ge-compound in benzene, refluxed for 2 h; org. layer extracted (Et2O), dried over Na2SO4, solvents removed in vacuo, recrystd. (pentane); elem. anal.;
DOI:10.1016/S0277-5387(00)86091-X