tris(methoxy)mesitylgermane

Base Information

Chemical Name:tris(methoxy)mesitylgermane
CAS No.:126529-82-6
Molecular Formula:C₁₂H₂₀GeO₃
Molecular Weight:284.879
Hs Code.:

Synonyms:tris(methoxy)mesitylgermane

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Chemical Property of tris(methoxy)mesitylgermane

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Technology Process of tris(methoxy)mesitylgermane

There total 2 articles about tris(methoxy)mesitylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 114806-82-5
(2,4,6-trimethylphenyl)trichlorogermane

: 126529-82-6
tris(methoxy)mesitylgermane

Guidance literature:: With methanol; triethyl amine; In benzene; byproducts: Et3N.HCl; Triethylamine was added to a mixt. of mesityl(trichloro)germane and methanol in benzene and heated to reflux for 2 h.; filtn. to eliminate Et3N.HCl, distn., elem. anal.;

Reference yield:

: 67-56-1
methanol

: 114806-82-5
(2,4,6-trimethylphenyl)trichlorogermane

: 126529-82-6
tris(methoxy)mesitylgermane

: bis(methoxy)mesitylchlorogermane

: 210487-91-5
methoxymesityldichlorogermane

Guidance literature:: With n-butyllithium; In hexane; benzene; byproducts: LiCl; inert atmosphere; dropwise addn. of equimolar amt. of LiOMe (prepd. fromBuLi (in hexane) and MeOH) to Ge-compd. (in C6H6, at room temp.), stir ring (room temp., 2 h); centrifugation off of LiCl, concn. (vac.); product mixt. not sepd., detd. by (1)H-NMR spectroscopy;
DOI:10.1016/S0020-1693(97)06137-9

Reference yield: 91.0%

: 126529-82-6
tris(methoxy)mesitylgermane

: 41823-71-6
bis(trimethylsilyl)methyllithium

: 136094-87-6
bisyl(mesityl)dimethoxygermane

Guidance literature:: In diethyl ether; pentane; byproducts: MeOLi; under inert gas, bisylLi in Et2O added to Ge-compound in pentane at -78°C, warmed to room temp., refluxed for 4 h; filtered, evaporated in vacuo, recrystd. (pentane); elem. anal.;
DOI:10.1016/S0277-5387(00)86091-X