N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide

Base Information

Chemical Name:N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide
CAS No.:220378-07-4
Molecular Formula:C₃₅H₃₆ClN₃O₂S
Molecular Weight:598.209
Hs Code.:

Synonyms:N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide

Chemical Property:

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Technology Process of N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide

There total 6 articles about N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 220378-07-4
N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide

Guidance literature:

Reference yield:

: N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hex-1-enesulfonamide

: 220378-07-4
N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1016/S0968-0896(01)00295-4

Reference yield:

: 42060-30-0
N-(4-chloro-benzyl)-methanesulfonamide

: 220378-07-4
N-(4-chlorobenzyl)-6-(1-(triphenylmethyl)imidazol-4-yl)-1-hexane sulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 89 percent / N,N-4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h

2.1: LDA / tetrahydrofuran / 1 h / -78 °C

2.2: tetrahydrofuran / 18 h / -78 - 20 °C

3.1: Cs₂CO₃ / methanol / 18 h / 20 °C

4.1: H₂ / 10 percent Pd/C / tetrahydrofuran / 18 h / 20 °C

With dmap; hydrogen; caesium carbonate; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/S0968-0896(01)00295-4