(S)-bis(acetato-O)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine

Base Information

• Chemical Name: (S)-bis(acetato-O)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine
• CAS No.: 215317-10-5
• Molecular Formula: C₁₄H₁₉IO₆
• Molecular Weight: 410.206
• Mol file: 215317-10-5.mol

Synonyms:(S)-bis(acetato-O)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine

Chemical Property of (S)-bis(acetato-O)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of (S)-bis(acetato-O)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine

There total 1 articles about (S)-bis(acetato-O)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

acetic acid (64-19-7,77671-22-8) + (S)-2-iodo-4-methoxy-(1-methoxyethyl)benzene (215316-98-6) → (S)-bis(acetato-O)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine (215317-10-5)

Guidance literature:

With sodium perborate; at 60 ℃; for 3h;

DOI:10.1021/jo980475x

Reference yield: 93.0%

toluene-4-sulfonic acid (104-15-4) + (S)-bis(acetato-O)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine (215317-10-5) → (S)-hydroxy(4-methylbenzenesulfonato-κO)[2-(1-methoxyethyl)-5-methoxyphenyl]iodine

Guidance literature:

In acetonitrile; for 1h;

DOI:10.1021/jo980475x

upstream raw materials:

acetic acid

(S)-2-iodo-4-methoxy-(1-methoxyethyl)benzene