p.tolyl ethanethioate de S-methyle

Base Information

Chemical Name:p.tolyl ethanethioate de S-methyle
CAS No.:17293-68-4
Molecular Formula:C₁₀H₁₂OS
Molecular Weight:180.271
Hs Code.:

Synonyms:p.tolyl ethanethioate de S-methyle

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Chemical Property of p.tolyl ethanethioate de S-methyle

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Technology Process of p.tolyl ethanethioate de S-methyle

There total 4 articles about p.tolyl ethanethioate de S-methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 91914-41-9
N-phenyl p-tolyl ethanethioimidate de methyle

: 17293-68-4
p.tolyl ethanethioate de S-methyle

Guidance literature:: With hydrogenchloride; water; In acetonitrile; at 50 ℃; for 6h;
DOI:10.1016/S0040-4020(01)91806-X

Reference yield:

: 29875-07-8
(4-methylbenzyl)magnesium chloride

: 17293-68-4
p.tolyl ethanethioate de S-methyle

Guidance literature:: Multi-step reaction with 2 steps

1: 2) HMPA / 1) THF, hexane, -10 degC, 2h, 2) room temperature, 16h,

2: 83 percent / H₂O, 10percent HCl / acetonitrile / 6 h / 50 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; water; In acetonitrile;
DOI:10.1016/S0040-4020(01)91806-X