N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide
• CAS No.: 1434622-86-2
• Molecular Formula: C₂₄H₂₇NO₅S
• Molecular Weight: 441.548

Synonyms:N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide

Chemical Property of N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide

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Technology Process of N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide

There total 2 articles about N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

(S)-N-(p-tolylsulfonyl)-2-phenylaziridine (24395-14-0,62596-62-7,151003-26-8,149769-84-6) + (3,4-dimethoxyphenyl)methanol (93-03-8) → N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide (1434622-86-2)

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In 1,2-dichloro-ethane; for 3h; Reflux;

DOI:10.1021/ol4008525

Reference yield: 61.0%

N-(p-tolylsulfonyl)-2-phenylaziridine (24395-14-0) + (3,4-dimethoxyphenyl)methanol (93-03-8) → N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide (1434622-86-2)

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In 1,2-dichloro-ethane; for 3h; Reflux;

DOI:10.1021/ol4008525

Reference yield: 72.0%

N-(2-(3,4-dimethoxybenzyloxy)-2-phenylethyl)-4-methylbenzenesulfonamide (1434622-86-2) → 6,7-dimethoxy-4-phenyl-2-tosyl-1,2,3,4-tetrahydroisoquinoline (1434621-80-3)

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In 1,2-dichloro-ethane; for 15h; Reflux;

DOI:10.1021/ol4008525

upstream raw materials:

(S)-N-(p-tolylsulfonyl)-2-phenylaziridine

(3,4-dimethoxyphenyl)methanol

N-(p-tolylsulfonyl)-2-phenylaziridine

Downstream raw materials:

6,7-dimethoxy-4-phenyl-2-tosyl-1,2,3,4-tetrahydroisoquinoline

N-(3,4-dimethoxybenzyl)-N-(2-hydroxy-2-phenylethyl)-4-methylbenzenesulfonamide

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