(1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester

Base Information

Chemical Name:(1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester
CAS No.:151059-55-1
Molecular Formula:C₁₉H₂₀O₅
Molecular Weight:328.365
Hs Code.:

Synonyms:(1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester

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Chemical Property of (1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester

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Technology Process of (1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester

There total 3 articles about (1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: (1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl ester, 2-(trimethylsilyl)ethyl ester

: 151059-55-1
(1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester

Guidance literature:: With tetraethylammonium fluoride; In acetonitrile; at 20 ℃;
DOI:10.1021/jf00035a038

Reference yield:

: 20416-09-5
(5-benzylfuran-3-yl)methanol

: 151059-55-1
(1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 1,3-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 0 - 20 °C

2: 61 percent / tetraethylammonium fluoride / acetonitrile / 20 °C

With dmap; tetraethylammonium fluoride; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1021/jf00035a038

Reference yield:

: 151059-51-7
(1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, 2-(trimethylsilyl)ethyl monoester

: 151059-55-1
(1R-trans)-2,2-dimethylcyclopropane-1,3-dicarboxylic acid, <2-(phenylmethyl)-4-furyl>methyl monoester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 1,3-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 0 - 20 °C

2: 61 percent / tetraethylammonium fluoride / acetonitrile / 20 °C

With dmap; tetraethylammonium fluoride; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1021/jf00035a038