4-nitro-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester)

Base Information

• Chemical Name: 4-nitro-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester)
• CAS No.: 38734-34-8
• Molecular Formula: C₁₇H₂₂N₂O₄
• Molecular Weight: 318.373
• Mol file: 38734-34-8.mol

Synonyms:4-nitro-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester)

Chemical Property of 4-nitro-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4-nitro-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester)

There total 2 articles about 4-nitro-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-nitro-benzoyl chloride (122-04-3) + lupinine (486-70-4) → 4-nitro-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester) (38734-34-8)

Guidance literature:

With triethylamine; In benzene; 1) 0 - 2 deg C, 40 min; 2) 2 --> 20 deg C, 3 h; 3) 70 deg C, 50 min;

DOI:10.1007/BF00954719

Reference yield:

→ Lupinin-(4-nitro-benzoat) (38734-34-8)

Guidance literature:

Lupinin, 1) 4-Nitro-benzoylchlorid/Bzl./Et3N, 2) Sdt. unter N2-Strom;

Reference yield:

4-nitro-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester) (38734-34-8) → 4-amino-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester) (38734-38-2)

Guidance literature:

With hydrogenchloride; tin;

upstream raw materials:

4-nitro-benzoyl chloride

lupinine

Downstream raw materials:

4-amino-benzoic acid-((9aR)-(9ar)-octahydroquinolizin-1t-ylmethyl ester)