Technology Process of C24H24N2O10
There total 6 articles about C24H24N2O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
In
dichloromethane;
for 18h;
Ambient temperature;
DOI:10.1021/ja00213a047
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 90 percent / (i-Bu)2AlH / diethyl ether / 4 h / Ambient temperature
2: 77 percent / toluene / 6 h / Heating
3: 1) KOH, MeOH 2) (i-Pr)2NEt / 1) reflux, 2 h. 2) CH2Cl2 room temperature, 4 h.
4: (i-Pr)2NLi-HMPA / tetrahydrofuran / 4 h / Ambient temperature
5: 90 percent / HCl / methanol / 0.5 h / Heating
6: 78 percent / DMAP, pyridine / CH2Cl2 / 18 h / Ambient temperature
With
pyridine; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; potassium hydroxide; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide;
hydrogenchloride;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ja00213a047
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 77 percent / toluene / 6 h / Heating
2: 1) KOH, MeOH 2) (i-Pr)2NEt / 1) reflux, 2 h. 2) CH2Cl2 room temperature, 4 h.
3: (i-Pr)2NLi-HMPA / tetrahydrofuran / 4 h / Ambient temperature
4: 90 percent / HCl / methanol / 0.5 h / Heating
5: 78 percent / DMAP, pyridine / CH2Cl2 / 18 h / Ambient temperature
With
pyridine; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; potassium hydroxide; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide;
hydrogenchloride;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja00213a047
