5-Chloro-3-(4-methylphenyl)-6-phenyl-1,2,4-triazine

Base Information

Chemical Name:5-Chloro-3-(4-methylphenyl)-6-phenyl-1,2,4-triazine
CAS No.:109306-99-2
Molecular Formula:C₁₆H₁₂ClN₃
Molecular Weight:281.744
Hs Code.:
DSSTox Substance ID:DTXSID801225556

Synonyms:5-Chloro-3-(4-methylphenyl)-6-phenyl-1,2,4-triazine;DTXSID801225556;109306-99-2

Suppliers and Price of 5-Chloro-3-(4-methylphenyl)-6-phenyl-1,2,4-triazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Chloro-3-(4-methylphenyl)-6-phenyl-1,2,4-triazine

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:281.0719751
Heavy Atom Count:20
Complexity:298

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2=NC(=C(N=N2)C3=CC=CC=C3)Cl

Technology Process of 5-Chloro-3-(4-methylphenyl)-6-phenyl-1,2,4-triazine

There total 3 articles about 5-Chloro-3-(4-methylphenyl)-6-phenyl-1,2,4-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 36993-96-1
6-phenyl-3-p-tolyl-1,2,4-triazin-5-one

: 109306-99-2
5-Chloro-6-phenyl-3-p-tolyl-[1,2,4]triazine

Guidance literature:: With phosphorus pentachloride; In toluene; for 24h; Heating;

Reference yield:

: 62230-47-1
p-methylbenzamidrazone

: 109306-99-2
5-Chloro-6-phenyl-3-p-tolyl-[1,2,4]triazine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / dimethylformamide / 1.) from 0 deg C to RT, 0.5 h, 2.) reflux, 3 h

2: POCl₃ / 2 h / Heating

With trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1021/jo00228a024

Reference yield:

: 611-73-4
Benzoylformic acid

: 109306-99-2
5-Chloro-6-phenyl-3-p-tolyl-[1,2,4]triazine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / dimethylformamide / 1.) from 0 deg C to RT, 0.5 h, 2.) reflux, 3 h

2: POCl₃ / 2 h / Heating

With trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1021/jo00228a024