C₂₅H₂₉N₃O₃*ClH

Base Information

Chemical Name:C₂₅H₂₉N₃O₃*ClH
CAS No.:1613625-31-2
Molecular Formula:C₂₅H₂₉N₃O₃*ClH
Molecular Weight:455.984
Hs Code.:

C<sub>25</sub>H<sub>29</sub>N<sub>3</sub>O<sub>3</sub>*ClH

Synonyms:C₂₅H₂₉N₃O₃*ClH

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Chemical Property of C₂₅H₂₉N₃O₃*ClH

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Technology Process of C₂₅H₂₉N₃O₃*ClH

There total 17 articles about C₂₅H₂₉N₃O₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15971-29-6
4-methoxy-1-naphthaldehyde

: 1613625-31-2
C₂₅H₂₉N₃O₃*ClH

Guidance literature:: Multi-step reaction with 18 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / 0 °C

1.2: 36 h / 20 °C

2.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C

4.2: 1.8 h / -78 - 20 °C

5.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

5.2: 0.08 h / -78 °C

5.3: 16 h / -78 - 24 °C

6.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.2 h / 0 - 20 °C

7.1: hydrogen; palladium 10% on activated carbon / water / 3 h / 20 °C / 760.05 Torr

8.1: acetic acid; hydrogen bromide / 3 h / Reflux

9.1: acetyl chloride / 4 h / 0 °C / Reflux

10.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C

11.1: pyridine / 2 h / 0 - 20 °C

12.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

13.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

14.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 2 h / 0 °C

15.1: ammonia / methanol / 18 h / 0 - 20 °C

16.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

17.1: sodium hydrogencarbonate / methanol; water / 0.17 h / 0 °C

17.2: 2 h / 0 - 20 °C

18.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; dichloromethane; cyclohexane; water; acetonitrile;

Reference yield:

: methyl-3-(4-methoxy-1-naphthyl)-E-propenoate

: 1613625-31-2
C₂₅H₂₉N₃O₃*ClH

Guidance literature:: Multi-step reaction with 17 steps

1.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

2.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C

3.2: 1.8 h / -78 - 20 °C

4.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

4.2: 0.08 h / -78 °C

4.3: 16 h / -78 - 24 °C

5.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.2 h / 0 - 20 °C

6.1: hydrogen; palladium 10% on activated carbon / water / 3 h / 20 °C / 760.05 Torr

7.1: acetic acid; hydrogen bromide / 3 h / Reflux

8.1: acetyl chloride / 4 h / 0 °C / Reflux

9.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C

10.1: pyridine / 2 h / 0 - 20 °C

11.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

12.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

13.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 2 h / 0 °C

14.1: ammonia / methanol / 18 h / 0 - 20 °C

15.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

16.1: sodium hydrogencarbonate / methanol; water / 0.17 h / 0 °C

16.2: 2 h / 0 - 20 °C

17.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; cyclohexane; water; acetonitrile;

Reference yield:

: 33189-02-5
β-(4-methoxy-1-naphthyl)propionic acid

: 1613625-31-2
C₂₅H₂₉N₃O₃*ClH

Guidance literature:: Multi-step reaction with 15 steps

1.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C

1.2: 1.8 h / -78 - 20 °C

2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

2.2: 0.08 h / -78 °C

2.3: 16 h / -78 - 24 °C

3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 1.2 h / 0 - 20 °C

4.1: hydrogen; palladium 10% on activated carbon / water / 3 h / 20 °C / 760.05 Torr

5.1: acetic acid; hydrogen bromide / 3 h / Reflux

6.1: acetyl chloride / 4 h / 0 °C / Reflux

7.1: sodium hydrogencarbonate / methanol; water / 1 h / 0 - 20 °C

8.1: pyridine / 2 h / 0 - 20 °C

9.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

10.1: sodium hydroxide; water / tetrahydrofuran; methanol / 2 h / 20 °C

11.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 2 h / 0 °C

12.1: ammonia / methanol / 18 h / 0 - 20 °C

13.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

14.1: sodium hydrogencarbonate / methanol; water / 0.17 h / 0 °C

14.2: 2 h / 0 - 20 °C

15.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; pivaloyl chloride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; cyclohexane; water; acetonitrile;