meso-3,3'-diaminohexestrol 4,4'-dimethyl ether

Base Information

Chemical Name:meso-3,3'-diaminohexestrol 4,4'-dimethyl ether
CAS No.:74536-59-7
Molecular Formula:C₂₀H₂₈N₂O₂
Molecular Weight:328.455
Hs Code.:

Synonyms:meso-3,3'-diaminohexestrol 4,4'-dimethyl ether

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Chemical Property of meso-3,3'-diaminohexestrol 4,4'-dimethyl ether

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Technology Process of meso-3,3'-diaminohexestrol 4,4'-dimethyl ether

There total 8 articles about meso-3,3'-diaminohexestrol 4,4'-dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 74536-58-6
meso-3,3'-dinitrohexestrol dimethyl ether

: 74536-59-7
meso-3,3'-diaminohexestrol 4,4'-dimethyl ether

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 12h; under 760 Torr;
DOI:10.1021/jm00183a007

Reference yield: 78.0%

: 74536-58-6
meso-3,4-Bis(4-methoxy-3-nitrophenyl)hexan

: 74536-59-7
meso-3,3'-(1,2-Diethylethylen)bis(6-methoxyanilin)

Guidance literature:: With hydrazine hydrate; nickel; for 1h; Heating;
DOI:10.1002/ardp.19813140711

Reference yield:

: 84-16-2,26614-21-1
hexestrol

: 74536-59-7
meso-3,3'-diaminohexestrol 4,4'-dimethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 14 percent / acetic anhydride, Cu(NO₃)2*3H₂O / acetic acid; tetrahydrofuran / 0.17 h

2: K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

3: 97 percent / H₂ / Pd/C (5percent) / tetrahydrofuran / 12 h / 760 Torr

With hydrogen; acetic anhydride; potassium carbonate; copper(II) nitrate; palladium on activated charcoal; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00183a007