(3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide

Base Information

Chemical Name:(3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide
CAS No.:152918-53-1
Molecular Formula:C₂₃H₂₇N₇O₅
Molecular Weight:481.511
Hs Code.:

Synonyms:(3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide

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Chemical Property of (3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide

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Technology Process of (3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide

There total 6 articles about (3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26177-43-5
3-nitrobenzylamine hydrochloride

: 152918-53-1
(3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / 5percent Pd/C / methanol / 0.75 h / 2585.7 Torr

2: Et₃N / ethanol / 12 h / 80 °C

3: Et₃N / dimethylformamide / 0.5 h

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00031a014

Reference yield:

: 104940-65-0
1'-deoxy-1'-(6-chloro-9H-purin-9-yl)2',3'-O-isopropylidene-β-D-ribofuranosyl chloride

: 152918-53-1
(3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 0.25 h / 10 °C

2: Et₃N / ethanol / 12 h / 80 °C

3: Et₃N / dimethylformamide / 0.5 h

With triethylamine; In ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00031a014

Reference yield:

: 152918-47-3
2',3'-isopropylidene-1-(6-chloro-9H-purin-9-yl)-1-deoxy-N-methyl-β-D-ribofuranosiduronamide

: 152918-53-1
(3aS,4S,6R,6aR)-6-[6-(3-Acetylamino-benzylamino)-purin-9-yl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole-4-carboxylic acid methylamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / ethanol / 12 h / 80 °C

2: Et₃N / dimethylformamide / 0.5 h

With triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00031a014