N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide

Base Information

Chemical Name:N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide
CAS No.:854133-12-3
Molecular Formula:C₁₆H₂₂FNO₃
Molecular Weight:295.354
Hs Code.:

<i>N</i>-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide

Synonyms:N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide

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Chemical Property of N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide

Chemical Property:

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Technology Process of N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide

There total 3 articles about N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52721-69-4
[2-(2-fluorophenyl)ethyl]amine

: 854133-03-2
2-(2-methyl-[1,3]dioxolan-2-yl)-butyryl chloride

: 854133-12-3
N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2005.03.054

Reference yield:

: 27773-10-0
carbethoxy-1 ethylene dioxy-2 ethyl-1 propane

: 854133-12-3
N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide

Guidance literature:: Multi-step reaction with 3 steps

1: aq. KOH / dioxane / 12 h / 35 °C

2: oxalyl chloride / CH₂Cl₂ / 2 h / 20 °C

3: pyridine / 12 h / 20 °C

With pyridine; potassium hydroxide; oxalyl dichloride; In 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2005.03.054

Reference yield:

: 751428-10-1
2-(2-methyl-[1,3]dioxolan-2-yl)-butyric acid

: 854133-12-3
N-[2-(2-fluoro-phenyl)-ethyl]-2-(2-methyl-[1,3]dioxolan-2-yl)-butyramide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂ / 2 h / 20 °C

2: pyridine / 12 h / 20 °C

With pyridine; oxalyl dichloride; In dichloromethane;
DOI:10.1016/j.bmcl.2005.03.054