C₂₂H₂₂N₆O₂S

Base Information

Chemical Name:C₂₂H₂₂N₆O₂S
CAS No.:1355249-49-8
Molecular Formula:C₂₂H₂₂N₆O₂S
Molecular Weight:434.522
Hs Code.:

C<sub>22</sub>H<sub>22</sub>N<sub>6</sub>O<sub>2</sub>S

Synonyms:C₂₂H₂₂N₆O₂S

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Chemical Property of C₂₂H₂₂N₆O₂S

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Technology Process of C₂₂H₂₂N₆O₂S

There total 7 articles about C₂₂H₂₂N₆O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 13036-57-2
2-chloro-4-methylpyrimidine

: 1355249-48-7
C₁₇H₁₈N₄O₂S

: 1355249-49-8
C₂₂H₂₂N₆O₂S

Guidance literature:: With caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 100 ℃; for 2h;

Reference yield:

: 1355249-29-4
ethyl 4-iodo-1-(4-methoxybenzyl)-1H-pyrazole-3-carboxylate

: 1355249-49-8
C₂₂H₂₂N₆O₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C

2.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 1.5 h / 80 °C / Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran / 2 h / Reflux

3.2: 20 °C

4.1: sulfuric acid / water / 0.25 h / 80 °C

4.2: pH 8

5.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 2 h / 100 °C

With potassium phosphate; lithium borohydride; n-butyllithium; sulfuric acid; caesium carbonate; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: 1355249-30-7
C₂₀H₂₇BN₂O₅

: 1355249-49-8
C₂₂H₂₂N₆O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 1.5 h / 80 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 2 h / Reflux

2.2: 20 °C

3.1: sulfuric acid / water / 0.25 h / 80 °C

3.2: pH 8

4.1: caesium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 2 h / 100 °C

With potassium phosphate; lithium borohydride; sulfuric acid; caesium carbonate; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;