2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid

Base Information

Chemical Name:2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid
CAS No.:485799-91-5
Molecular Formula:C₂₇H₂₁NO₄
Molecular Weight:423.468
Hs Code.:

Synonyms:2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid

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Chemical Property of 2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid

Chemical Property:

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Technology Process of 2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid

There total 6 articles about 2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-[3-(4'-cyano-biphenyl-4-yloxy)-propoxy]-naphthalene-1-carboxylic acid benzyl ester

: 485799-91-5
2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid

Guidance literature:: With hydrogen; 10percent Pd/C; In tetrahydrofuran;
DOI:10.1021/jm020160g

Reference yield:

: 86170-47-0
2-hydroxynaphthalene-1-carboxylic acid benzyl ester

: 485799-91-5
2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃ / dimethylformamide / 3 h / 55 °C

2: Ba(OH)2*8H₂O / methanol / 15 h / 20 °C

3: Et₃N / CH₂Cl₂ / 18 h / 40 °C

4: K₂CO₃ / dimethylformamide / 3 h / 60 °C

5: H₂ / 10percent Pd/C / tetrahydrofuran

With barium dihydroxide; hydrogen; potassium carbonate; triethylamine; 10percent Pd/C; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020160g

Reference yield:

: 485799-90-4
2-(3-hydroxypropoxy)naphthalene-1-carboxylic acid benzyl ester

: 485799-91-5
2-[2-[(4'-cyano[1,1'-biphenyl]-4-yl)oxy]propyloxy]-N-hydroxy-1-naphthalenecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 18 h / 40 °C

2: K₂CO₃ / dimethylformamide / 3 h / 60 °C

3: H₂ / 10percent Pd/C / tetrahydrofuran

With hydrogen; potassium carbonate; triethylamine; 10percent Pd/C; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm020160g