(S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane

Base Information

Chemical Name:(S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane
CAS No.:205380-74-1
Molecular Formula:C₁₆H₂₈O₂Si
Molecular Weight:280.483
Hs Code.:

Synonyms:(S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane

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Chemical Property of (S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane

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Technology Process of (S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane

There total 8 articles about (S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 205380-73-0
(S)-2-benzyl-3-((tert-butyldimethylsilyl)oxy)-propyl acetate

: 205380-74-1
(S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane

Guidance literature:: With sodium carbonate; In methanol; at 20 ℃;
DOI:10.1002/ejoc.200800334

Reference yield:

: 110270-49-0
(R)-3-acetoxy-2-benzyl-1-propanol

: 205380-74-1
(S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / triethylamine / CH₂Cl₂ / 24 h

2: 89 percent / H₂O; K₂CO₃ / methanol / 1.5 h

With water; potassium carbonate; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2006.06.045

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 205380-74-1
(S)-2-benzyl-3-hydroxypropoxy tert-butyl dimethyl silane

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / triethylamine / CH₂Cl₂ / 24 h

2: 89 percent / H₂O; K₂CO₃ / methanol / 1.5 h

With water; potassium carbonate; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2006.06.045