tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside

Base Information

Chemical Name:tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside
CAS No.:565462-98-8
Molecular Formula:C₃₀H₃₄O₆S
Molecular Weight:522.662
Hs Code.:

Synonyms:tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside

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Chemical Property of tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside

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Technology Process of tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside

There total 5 articles about tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 76-83-5
trityl chloride

: 453524-96-4
tetrahydropyran-2-yl 5-deoxy-5-thio-α-D-glucopyranoside

: 565462-98-8
tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside

Guidance literature:: With pyridine; dmap; at 20 ℃; for 24h;
DOI:10.1016/j.bmc.2005.05.028

Reference yield:

: 137886-82-9
2,3,4,6-Tetra-O-acetyl-5-thio-α-D-glucopyranose

: 565462-98-8
tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / p-TsOH / CH₂Cl₂ / 1.5 h / 0 °C

2: 82 percent / NaOMe / methanol / 3.5 h / 20 °C

3: 80 percent / 4-(dimethylamino)pyridine; pyridine / 24 h / 20 °C

With pyridine; dmap; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2005.05.028

Reference yield:

: 453525-11-6
tetrahydropyran-2-yl 2,3,4,6-tetra-O-acetyl-5-deoxy-5-thio-α-D-glucopyranoside

: 565462-98-8
tetrahydropyran-2-yl 6-O-triphenylmethyl-5-deoxy-5-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / NaOMe / methanol / 3.5 h / 20 °C

2: 80 percent / 4-(dimethylamino)pyridine; pyridine / 24 h / 20 °C

With pyridine; dmap; sodium methylate; In methanol;
DOI:10.1016/j.bmc.2005.05.028