N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine

Base Information

Chemical Name:N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine
CAS No.:240807-24-3
Molecular Formula:C₄₁H₅₃NO₄Si₂
Molecular Weight:680.047
Hs Code.:

Synonyms:N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine

Chemical Property:

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Technology Process of N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine

There total 4 articles about N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 105-36-2
ethyl bromoacetate

: 240807-21-0
(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine

: 240807-24-3
N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine

Guidance literature:: With potassium carbonate; In acetonitrile; for 38h; Ambient temperature;
DOI:10.1016/S0957-4166(99)00186-X

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 240807-24-3
N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / imidazole / CH₂Cl₂ / 36 h / Ambient temperature

2: 90 percent / H₂ / Pd(OH)2/C / methanol / 64 h / Ambient temperature

3: 90 percent / K₂CO₃ / acetonitrile / 38 h / Ambient temperature

With 1H-imidazole; hydrogen; potassium carbonate; palladium dihydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0957-4166(99)00186-X

Reference yield:

: 168647-93-6
(2S,4S)-1-<(S)-1-phenylethyl>-2,4-bis(hydroxymethyl)azetidine

: 240807-24-3
N-(ethoxycarbonylmethyl)-(S,S)-2,4-bis<(tert-butyldiphenylsiloxy)methyl>azetidine

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / imidazole / CH₂Cl₂ / 36 h / Ambient temperature

2: 90 percent / H₂ / Pd(OH)2/C / methanol / 64 h / Ambient temperature

3: 90 percent / K₂CO₃ / acetonitrile / 38 h / Ambient temperature

With 1H-imidazole; hydrogen; potassium carbonate; palladium dihydroxide; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0957-4166(99)00186-X