{N(CH₂CH₃)4}⁽¹⁺⁾*{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}^(1-)={N(CH₂CH₃)4}{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}

Base Information

• Chemical Name: {N(CH₂CH₃)4}⁽¹⁺⁾*{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}^(1-)={N(CH₂CH₃)4}{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}
• CAS No.: 80612-39-1
• Molecular Formula: C₈H₂₀N*C₃₉H₃₀FeO₃PSn
• Molecular Weight: 882.45

Synonyms:{N(CH₂CH₃)4}⁽¹⁺⁾*{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}^(1-)={N(CH₂CH₃)4}{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}

Chemical Property of {N(CH₂CH₃)4}⁽¹⁺⁾*{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}^(1-)={N(CH₂CH₃)4}{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}

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Technology Process of {N(CH₂CH₃)4}⁽¹⁺⁾*{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}^(1-)={N(CH₂CH₃)4}{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}

There total 2 articles about {N(CH₂CH₃)4}⁽¹⁺⁾*{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)}^(1-)={N(CH₂CH₃)4}{((C₆H₅)3Sn)Fe(CO)3(P(C₆H₅)3)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

K2[Fe(CO)3(PPh3)] (80612-34-6) + triphenyltin chloride (639-58-7) → {N(CH2CH3)4}(1+)*{((C6H5)3Sn)Fe(CO)3(P(C6H5)3)}(1-)={N(CH2CH3)4}{((C6H5)3Sn)Fe(CO)3(P(C6H5)3)} (80612-39-1)

Guidance literature:

In tetrahydrofuran; elem. anal.;

DOI:10.1021/ja00368a059

Reference yield: 65.0%

K2[Fe(CO)3(PPh3)] (80612-34-6) + tetraethylammonium bromide (71-91-0) + triphenyltin chloride (639-58-7) → {N(CH2CH3)4}(1+)*{((C6H5)3Sn)Fe(CO)3(P(C6H5)3)}(1-)={N(CH2CH3)4}{((C6H5)3Sn)Fe(CO)3(P(C6H5)3)} (80612-39-1)

Guidance literature:

In tetrahydrofuran; acetonitrile; adding dropwise THF soln. of Ph3SnCl to slurry of K2(Fe(CO)3(PPh3)) in THF (vigorous stirring), reacting (1.5 h), filtering, evapg. to dryness, redissolving , adding (Et4N)Br in CH3CN; removing solvent (vacuum), recrystn. (acetone-hexane), washing (EtOH, 2x), recrystn. (acetone-ether); elem. anal.;

upstream raw materials:

K₂[Fe(CO)3(PPh₃)]

tetraethylammonium bromide

triphenyltin chloride

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