(2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

Base Information

Chemical Name:(2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester
CAS No.:557793-29-0
Molecular Formula:C₅₈H₄₅N₉O₆P₄S₃
Molecular Weight:1184.15
Hs Code.:

(2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

Synonyms:(2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

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Chemical Property of (2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

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Technology Process of (2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

There total 1 articles about (2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3328-57-2
sodium 4-cyanophenolate

: 264869-56-9
C₃₀H₂₉Cl₄N₅O₂P₄S₃

: 557793-29-0
(2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1055/s-2003-37356

Reference yield: 95.0%

: 60-34-4
methylhydrazine

: 557793-29-0
(2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

: 557793-30-3
(2E,2E')-2,2'-[({[2-(1-methylhydrazino)ethyl]diphenylphosphoranylidene}amino)phosphinothioylidene]bis(oxy-1,4-phenylenemethylidyne)bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1055/s-2003-37356

Reference yield:

: 557793-29-0
(2E,2E')-2,2'-({[(ethenyldiphenylphosphoranylidene)amino]phosphinothioylidene}bis(oxy-1,4-phenylenemethylidyne))bis-1-methyl-phosphorohydrazidothioic acid O,O,O,O-tetrakis(4-cyanophenyl) ester

: C₆₆H₅₅N₁₁O₈P₄S₃

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / tetrahydrofuran / 3 h / 20 °C

2: 95 percent / tetrahydrofuran / 24 h / 20 °C

In tetrahydrofuran;
DOI:10.1055/s-2003-37356