Technology Process of C18H13F3O4Te
There total 6 articles about C18H13F3O4Te which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) magnesium, iodine, 2.) tellurium / 1.) THF, reflux, 2.) reflux, 3 h
2: 1.) sodium borohydride / 1.) THF, ethanol, 2.) room temperature, 0.5 h
3: 89 percent / aq. potassium hydroxide / ethanol / 1 h / 50 °C
4: oxalyl chloride
5: 96 percent / aluminum chloride / CH2Cl2 / -78 deg C -> room temperature
6: 50 percent / benzene / 1 h / Ambient temperature
With
potassium hydroxide; tellurium; sodium tetrahydroborate; aluminium trichloride; oxalyl dichloride; iodine; magnesium;
In
ethanol; dichloromethane; benzene;
DOI:10.1021/ja00342a040
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) sodium borohydride / 1.) THF, ethanol, 2.) room temperature, 0.5 h
2: 89 percent / aq. potassium hydroxide / ethanol / 1 h / 50 °C
3: oxalyl chloride
4: 96 percent / aluminum chloride / CH2Cl2 / -78 deg C -> room temperature
5: 50 percent / benzene / 1 h / Ambient temperature
With
potassium hydroxide; sodium tetrahydroborate; aluminium trichloride; oxalyl dichloride;
In
ethanol; dichloromethane; benzene;
DOI:10.1021/ja00342a040