1-Fluoro-2-(4-iodobutyl)benzene

Base Information

Chemical Name:1-Fluoro-2-(4-iodobutyl)benzene
CAS No.:249922-30-3
Molecular Formula:C₁₀H₁₂FI
Molecular Weight:278.108
Hs Code.:
DSSTox Substance ID:DTXSID101303418
Nikkaji Number:J1.169.963D

Synonyms:1-fluoro-2-(4-iodobutyl)benzene;249922-30-3;SCHEMBL9476165;DTXSID101303418;AB93468;F80820

Suppliers and Price of 1-Fluoro-2-(4-iodobutyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Acrotein
1-Fluoro-2-(4-iodobutyl)benzene 97%
1g
$ 513.33

ACHEMBLOCK
1-Fluoro-2-(4-iodobutyl)benzene 97%
1G
$ 555.00

Total 2 raw suppliers

Chemical Property of 1-Fluoro-2-(4-iodobutyl)benzene

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:277.99678
Heavy Atom Count:12
Complexity:116

Purity/Quality:

95%-98% ^*data from raw suppliers

1-Fluoro-2-(4-iodobutyl)benzene 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CCCCI)F

Technology Process of 1-Fluoro-2-(4-iodobutyl)benzene

There total 4 articles about 1-Fluoro-2-(4-iodobutyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1033603-19-8
methanesulfonic acid 4-(2-fluoro-phenyl)-butyl ester

: 249922-30-3
2-fluoro-1-(4-iodobutyl)benzene

Guidance literature:: With sodium iodide; In acetone;
DOI:10.1016/S0040-4039(99)01434-3

Reference yield:

: 462-06-6
fluorobenzene

: 249922-30-3
2-fluoro-1-(4-iodobutyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: n-BuLi; KOt-Bu; HMPA / tetrahydrofuran / -85 - -40 °C

2: PPTS / ethanol

3: Et₃N / CH₂Cl₂

4: NaI / acetone

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; potassium tert-butylate; pyridinium p-toluenesulfonate; triethylamine; sodium iodide; In tetrahydrofuran; ethanol; dichloromethane; acetone; 1: Substitution / 2: de-tetrahydropyranylation / 3: mesylation / 4: Substitution;
DOI:10.1016/S0040-4039(99)01434-3

Reference yield:

: 249922-28-9
4-(2-fluorophenyl)butan-1-ol

: 249922-30-3
2-fluoro-1-(4-iodobutyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: NaI / acetone

With triethylamine; sodium iodide; In dichloromethane; acetone; 1: mesylation / 2: Substitution;
DOI:10.1016/S0040-4039(99)01434-3