(S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)-N₆-[(dimethylamino)methylene]adenine

Base Information

• Chemical Name: (S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)-N₆-[(dimethylamino)methylene]adenine
• CAS No.: 1159174-76-1
• Molecular Formula: C₃₂H₃₄N₆O₄
• Molecular Weight: 566.66

Synonyms:(S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)-N₆-[(dimethylamino)methylene]adenine

Chemical Property of (S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)-N₆-[(dimethylamino)methylene]adenine

Chemical Property:

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Technology Process of (S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)-N₆-[(dimethylamino)methylene]adenine

There total 1 articles about (S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)-N₆-[(dimethylamino)methylene]adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)adenine (851050-21-0) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → (S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)-N6-[(dimethylamino)methylene]adenine (1159174-76-1)

Guidance literature:

In N,N-dimethyl-formamide; at 60 ℃; for 1h;

DOI:10.1021/jo900365a

Reference yield: 83.0%

(S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)-N6-[(dimethylamino)methylene]adenine (1159174-76-1) + N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite (102691-36-1) → C41H51N8O5P (1159174-79-4)

Guidance literature:

With 4,5-dicyano-1H-imidazole; In dichloromethane; acetonitrile; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo900365a

upstream raw materials:

(S)-9-(3-(4,4'-dimethoxytrityloxy)-2-hydroxypropyl)adenine

N,N-dimethyl-formamide dimethyl acetal

Downstream raw materials:

C₄₁H₅₁N₈O₅P

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