4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

Base Information

Chemical Name:4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl
CAS No.:692205-36-0
Molecular Formula:C₇₀H₇₆Br₂O₁₀
Molecular Weight:1237.18
Hs Code.:

4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

Synonyms:4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

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Chemical Property of 4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

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Technology Process of 4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

There total 21 articles about 4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 100886-40-6
4'-Methoxymethoxy-biphenyl-4-ol

: 692205-13-3
5-(3-{3-[3-Benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-bromomethyl-phenoxymethyl)-2-bromo-1-(3-bromo-benzyloxy)-3-decyloxy-benzene

: 692205-36-0
4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 12h; Heating;
DOI:10.1021/jo049878p

Reference yield:

: 2050-77-3
Iododecane

: 692205-36-0
4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

2: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

3: 87 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

4: potassium carbonate; 18-crown-6 / tetrahydrofuran / 12 h / Heating

5: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

6: 90 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

7: 96 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

8: 96 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

With N-Bromosuccinimide; 18-crown-6 ether; dimethylsulfide borane complex; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1021/jo049878p

Reference yield:

: 92-88-6
4,4'-Dihydroxybiphenyl

: 692205-36-0
4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / NaH / tetrahydrofuran

2: 96 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

With 18-crown-6 ether; sodium hydride; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1021/jo049878p