4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol

Base Information

Chemical Name:4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol
CAS No.:692205-40-6
Molecular Formula:C₆₈H₇₂Br₂O₉
Molecular Weight:1193.12
Hs Code.:

Synonyms:4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol

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Chemical Property of 4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol

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Technology Process of 4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol

There total 23 articles about 4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 692205-36-0
4-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-4'-methoxymethoxy-biphenyl

: 692205-40-6
4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol

Guidance literature:: With methanol; toluene-4-sulfonic acid; In 1,4-dioxane; Heating;
DOI:10.1021/jo049878p

Reference yield:

: 2050-77-3
Iododecane

: 692205-40-6
4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol

Guidance literature:: Multi-step reaction with 9 steps

1: potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

2: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

3: 87 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

4: potassium carbonate; 18-crown-6 / tetrahydrofuran / 12 h / Heating

5: borane-dimethyl sulfide complex / tetrahydrofuran / 8 h / Heating

6: 90 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

7: 96 percent / triphenylphosphine; N-bromosuccinimide / tetrahydrofuran / 20 °C

8: 96 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

9: 80 percent / methanol; p-toluenesulfonic acid / dioxane / Heating

With methanol; N-Bromosuccinimide; 18-crown-6 ether; dimethylsulfide borane complex; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; acetone;
DOI:10.1021/jo049878p

Reference yield:

: 92-88-6
4,4'-Dihydroxybiphenyl

: 692205-40-6
4'-{3-{3-[3-benzyloxymethyl-5-(3-methyl-benzyloxy)-phenoxy]-propoxy}-5-[4-bromo-3-(3-bromo-benzyloxy)-5-decyloxy-benzyloxy]-benzyloxy}-biphenyl-4-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 31 percent / NaH / tetrahydrofuran

2: 96 percent / potassium carbonate; 18-crown-6 / acetone / 12 h / Heating

3: 80 percent / methanol; p-toluenesulfonic acid / dioxane / Heating

With methanol; 18-crown-6 ether; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; 1,4-dioxane; acetone;
DOI:10.1021/jo049878p