dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate

Base Information

Chemical Name:dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate
CAS No.:858108-90-4
Molecular Formula:C₃₂H₄₀NO₈P
Molecular Weight:597.645
Hs Code.:

Synonyms:dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate

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Chemical Property of dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate

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Technology Process of dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate

There total 8 articles about dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,3S,4R,5S,6R)-3-Azido-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-carbaldehyde

: 858108-90-4
dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate

Guidance literature:: Multi-step reaction with 6 steps

1: aq. NaBH₄ / tetrahydrofuran / 20 °C

2: PPh₃ / tetrahydrofuran / 20 °C

3: methanol / 20 °C

4: 88 percent / pyridine / CH₂Cl₂ / 20 °C

5: NaI / butan-2-one / 100 °C

6: 100 °C

With pyridine; sodium tetrahydroborate; triphenylphosphine; sodium iodide; In tetrahydrofuran; methanol; dichloromethane; butanone;
DOI:10.1055/s-2005-865226

Reference yield:

: 858108-82-4
C-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanol

: 858108-90-4
dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate

Guidance literature:: Multi-step reaction with 5 steps

1: PPh₃ / tetrahydrofuran / 20 °C

2: methanol / 20 °C

3: 88 percent / pyridine / CH₂Cl₂ / 20 °C

4: NaI / butan-2-one / 100 °C

5: 100 °C

With pyridine; triphenylphosphine; sodium iodide; In tetrahydrofuran; methanol; dichloromethane; butanone;
DOI:10.1055/s-2005-865226

Reference yield:

: ((2S,3R,4R,5S,6R)-3-Amino-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-methanol

: 858108-90-4
dimethyl C-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-α-D-mannopyranosyl)methanephosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / 20 °C

2: 88 percent / pyridine / CH₂Cl₂ / 20 °C

3: NaI / butan-2-one / 100 °C

4: 100 °C

With pyridine; sodium iodide; In methanol; dichloromethane; butanone;
DOI:10.1055/s-2005-865226