Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

Base Information

Chemical Name:Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate
CAS No.:1228361-05-4
Molecular Formula:C₃₃H₄₄O₅
Molecular Weight:520.709
Hs Code.:

Δ<sup>4</sup>/Δ<sup>1,4</sup>-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

Synonyms:Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

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Chemical Property of Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

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Technology Process of Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

There total 3 articles about Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1228360-87-9
methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

: 1228361-05-4
Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

Guidance literature:: With 2-iodoxybenzoic acid; trifluoroacetic acid; In dimethyl sulfoxide; at 60 ℃; Darkness;
DOI:10.1002/anie.201307465

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 14773-00-3
methyl (5β,7α)-12-hydroxy-3-oxo-cholan-24-oate

: 1228361-05-4
Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 20 °C

1.2: 0 °C

2.1: 2-iodoxybenzoic acid; trifluoroacetic acid / dimethyl sulfoxide / 60 °C / Darkness

With 2-iodoxybenzoic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/anie.201307465

Reference yield:

: 474-25-9
chenodeoxycholic acid

: 1228361-05-4
Δ⁴/Δ^1,4-methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene; methanol; diethyl ether / 0.33 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 20 °C

2.2: 0 °C

3.1: 2-iodoxybenzoic acid; trifluoroacetic acid / dimethyl sulfoxide / 60 °C / Darkness

With 2-iodoxybenzoic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1002/anie.201307465