3-Hydroxypropyl methacrylate

Base Information

• Chemical Name: 3-Hydroxypropyl methacrylate
• CAS No.: 2761-09-3
• Molecular Formula: C7H12 O3
• Molecular Weight: 144.17
• European Community (EC) Number: 220-426-2
• UNII: 523A6318HJ
• DSSTox Substance ID: DTXSID0062630
• Nikkaji Number: J101.364E
• Wikidata: Q27260952
• Mol file: 2761-09-3.mol

Synonyms:3-Hydroxypropyl methacrylate;2761-09-3;3-hydroxypropyl 2-methylprop-2-enoate;2-Propenoic acid, 2-methyl-, 3-hydroxypropyl ester;1,3-Propylene glycol methacrylate;Methacrylic Acid Hydroxypropyl Ester;523A6318HJ;Methacrylic acid, 3-hydroxypropyl ester;3-HYDROXYPROPYLMETHACRYLATE;hydroxypropylmethacrylate;SCHEMBL15480;3-METHACRYLOYLOXYPROPANOL;DTXSID0062630;UNII-523A6318HJ;1,3-propanediol monomethacrylate;3-Hydroxypropyl 2-methylacrylate #;AMY18806;(C3-H6-O)mult-C4-H6-O2;EINECS 220-426-2;AKOS024437764;AS-68327;Propenoic acid, 2-methyl-, hydroxypropyl ester;Q27260952

Chemical Property of 3-Hydroxypropyl methacrylate

Chemical Property:

• Vapor Pressure: 0.0363mmHg at 25°C
• Boiling Point: 213.5°Cat760mmHg
• PKA: 14.66±0.10(Predicted)
• Flash Point: 96.7°C
• PSA: 46.53000
• Density: 1.03g/cm³
• LogP: 0.48810
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 144.078644241
• Heavy Atom Count: 10
• Complexity: 129

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C)C(=O)OCCCO

Technology Process of 3-Hydroxypropyl methacrylate

There total 8 articles about 3-Hydroxypropyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,3-Epoxypropyl methacrylate (106-91-2,25067-05-4,98104-93-9) → 2-methylacrylic acid 3-hydroxypropyl ester (2761-09-3)

Guidance literature:

With chloroaluminium tetrahydroborate on poly(4-vinylpyridine); In ethanol; for 7h; Heating;

DOI:10.1039/a703327c

Reference yield: 92.0%

methacryloyl anhydride (760-93-0) + trimethyleneglycol (504-63-2) → 2-methylacrylic acid 3-hydroxypropyl ester (2761-09-3)

Guidance literature:

With triethylamine; In chloroform; at 30 ℃; Inert atmosphere;

DOI:10.1002/anie.201811848

Reference yield: 60.0%

sodium methacrylate (5536-61-8) + 1-chloro-3-hydroxypropane (627-30-5) → 2-methylacrylic acid 3-hydroxypropyl ester (2761-09-3)

Guidance literature:

With Aliquat 336; In acetonitrile; for 24h; Reflux;

DOI:10.1007/s00706-008-0045-y

upstream raw materials:

poly(methacrylic acid)

trimethyleneglycol

2,3-Epoxypropyl methacrylate

Methacryloyl chloride

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