N⁶-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine

Base Information

• Chemical Name: N⁶-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine
• CAS No.: 138571-50-3
• Molecular Formula: C₂₁H₁₉N₅O₄
• Molecular Weight: 405.413

Synonyms:N⁶-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine

Chemical Property of N⁶-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N⁶-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine

There total 4 articles about N⁶-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6-benzoyl-9-<(1R,2S,3R)-2,3-(isopropylidenedioxy)-4-(hydroxymethyl)-4-cyclopenten-1-yl>adenine (138571-49-0) → N6-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine (138571-50-3)

Guidance literature:

With barium permanganate; In 1,2-dichloro-ethane; for 3h; Heating;

DOI:10.1021/jm00080a018

Reference yield:

neplanocin A (72877-50-0,156407-85-1) → N6-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine (138571-50-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) trimethylsilyl chloride / 1.) pyridine, RT, 15 min, 2.) pyridine, RT, 2 h

2: 77 percent / 70percent HClO₄ / 3 h / Ambient temperature

3: BaMnO₄ / 1,2-dichloro-ethane / 3 h / Heating

With chloro-trimethyl-silane; perchloric acid; barium permanganate; In 1,2-dichloro-ethane;

DOI:10.1021/jm00080a018

Reference yield:

benzoyl chloride (98-88-4) → N6-benzoyl-9<(1R,2S,3R)-4-formyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine (138571-50-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) trimethylsilyl chloride / 1.) pyridine, RT, 15 min, 2.) pyridine, RT, 2 h

2: 77 percent / 70percent HClO₄ / 3 h / Ambient temperature

3: BaMnO₄ / 1,2-dichloro-ethane / 3 h / Heating

With chloro-trimethyl-silane; perchloric acid; barium permanganate; In 1,2-dichloro-ethane;

DOI:10.1021/jm00080a018

upstream raw materials:

N⁶-benzoyl-9-<(1R,2S,3R)-2,3-(isopropylidenedioxy)-4-(hydroxymethyl)-4-cyclopenten-1-yl>adenine

neplanocin A

benzoyl chloride

N⁶-benzoyl-9-<(1R,2S,3R)-2,3-dihydroxy-4-(hydroxymethyl)-4-cyclopenten-1-yl>adenine

Downstream raw materials:

N⁶-benzoyl-9<(1R,2S,3R)-4-(1-hydroxyethyl)-2,3-(isopropylidenodioxy)-4-cyclopenten-1-yl>adenine

N⁶-benzoyl-9<(1R,2S,3R)-4-ethenyl-2,3-(isopropylidenedioxy)-4-cyclopenten-1-yl>adenine

(3aR,6R,6aS)-6-(6-Benzoylamino-purin-9-yl)-2,2-dimethyl-6,6a-dihydro-3aH-cyclopenta[1,3]dioxole-4-carboxylic acid amide

(3aR,6R,6aS)-6-(6-Benzoylamino-purin-9-yl)-2,2-dimethyl-6,6a-dihydro-3aH-cyclopenta[1,3]dioxole-4-carboxylic acid methylamide

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