C₃₃H₄₆N₄O₃

Base Information

Chemical Name:C₃₃H₄₆N₄O₃
CAS No.:1613707-30-4
Molecular Formula:C₃₃H₄₆N₄O₃
Molecular Weight:546.753
Hs Code.:

C<sub>33</sub>H<sub>46</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₃₃H₄₆N₄O₃

Suppliers and Price of C₃₃H₄₆N₄O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₄₆N₄O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₄₆N₄O₃

There total 15 articles about C₃₃H₄₆N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (Z)-methyl 2-(tert-butyloxycarbonyl)amino-3-(1-(tert-butyldimethylsilyloxy)naphthalen-4-yl)acrylate

: 1613707-30-4
C₃₃H₄₆N₄O₃

Guidance literature:: Multi-step reaction with 8 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C / 760.05 Torr

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C

3: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

4: pyridine / 2 h / 0 - 20 °C

5: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

6: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

7: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

8: palladium 10% on activated carbon; hydrogen; acetic acid / methanol / 12 h / 20 °C / 760.05 Torr

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; water; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;

Reference yield:

: 1613707-21-3
methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldimethylsilyloxy)naphthalen-1-yl)propanoate

: 1613707-30-4
C₃₃H₄₆N₄O₃

Guidance literature:: Multi-step reaction with 7 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C

2: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

3: pyridine / 2 h / 0 - 20 °C

4: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

5: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

6: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

7: palladium 10% on activated carbon; hydrogen; acetic acid / methanol / 12 h / 20 °C / 760.05 Torr

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; water; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;

Reference yield:

: 1613707-22-4
methyl 2-(tert-butoxycarbonylamino)-3-(4-hydroxynaphthalen-1-yl)propanoate

: 1613707-30-4
C₃₃H₄₆N₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

2: pyridine / 2 h / 0 - 20 °C

3: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

4: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

5: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

6: palladium 10% on activated carbon; hydrogen; acetic acid / methanol / 12 h / 20 °C / 760.05 Torr

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; water; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;