(S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid

Base Information

Chemical Name:(S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid
CAS No.:1300040-41-8
Molecular Formula:C₁₃H₁₁NO₅
Molecular Weight:261.234
Hs Code.:

Synonyms:(S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid

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Chemical Property of (S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid

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Technology Process of (S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid

There total 1 articles about (S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228555-64-3
C₁₃H₉NO₅

: 1300040-41-8
(S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid

Guidance literature:: C₁₃H₉NO₅; With (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; at -40 - -10 ℃; for 12h; Inert atmosphere;

With water; In tetrahydrofuran; enantioselective reaction; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.ejmech.2011.02.039

Reference yield: 82.0%

: 1300040-41-8
(S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid

: 20445-31-2
R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid

: 1300040-37-2
4-hydroxy-2-oxo-6-((S)-phenyl((R)-3,3,3-trifluoro-2-methoxy-2-phenylpropanoyloxy) methyl)-1,2-dihydropyridine-3-carboxylic acid

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 6h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.02.039

Reference yield:

: 503-74-2
3-methylbutyric acid

: 1300040-41-8
(S)-4-hydroxy-6-(hydroxy(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid

: 663891-81-4
(S)-(+)-4-hydroxy-6-((3-methylbutanoyloxy)(phenyl)methyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; at 10 - 20 ℃; for 12h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.02.039