4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine

Base Information Edit

Chemical Name:4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine
CAS No.:106693-44-1
Molecular Formula:C₈H₁₅N₃O₃
Molecular Weight:201.225
Hs Code.:
Mol file:106693-44-1.mol

Synonyms:4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine

Suppliers and Price of 4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-Butyl3-Oxopyrazolidin-4-ylcarbamate
10mg
$ 90.00

Crysdot
tert-Butyl(3-oxopyrazolidin-4-yl)carbamate 95+%
1g
$ 806.00

American Custom Chemicals Corporation
TERT-BUTYL 3-OXOPYRAZOLIDIN-4-YLCARBAMATE 95.00%
5MG
$ 504.71

AK Scientific
tert-ButylN-(3-oxopyrazolidin-4-yl)carbamate
250mg
$ 343.00

aablocks
tert-Butyln-(3-oxopyrazolidin-4-yl)carbamate 95%
1g
$ 857.00

aablocks
tert-Butyln-(3-oxopyrazolidin-4-yl)carbamate 95%
250mg
$ 383.00

Total 0 raw suppliers

Chemical Property of 4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine Edit

Chemical Property:

Density:1.20±0.1 g/cm3(Predicted)

Purity/Quality:: tert-Butyl3-Oxopyrazolidin-4-ylcarbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine

There total 5 articles about 4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 55477-80-0
methyl 2-[(tert-butoxycarbonyl)amino]acrylate

: 106693-44-1
4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine

Guidance literature:: With hydrazine hydrate; In ethanol;
DOI:10.1016/S0040-4020(01)85956-1

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 106693-44-1
4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CHCl₃ / 0.5 h / 0 °C

2: DBU / CHCl₃ / 3 h / 0 °C

3: 49 percent / hydrazine hydrate / ethanol

With hydrazine hydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In ethanol; chloroform;
DOI:10.1016/S0040-4020(01)85956-1

Reference yield:

: 119542-95-9
2-tert-butoxycarbonylamino-3-chloro-propionic acid methyl ester

: 106693-44-1
4-(R,S)-(t-butoxycarbonylamino)-3-oxo-1,2-diazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: DBU / CHCl₃ / 3 h / 0 °C

2: 49 percent / hydrazine hydrate / ethanol

With hydrazine hydrate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol; chloroform;
DOI:10.1016/S0040-4020(01)85956-1