C₃₅H₄₈Cl₂N₂O₃

Base Information

Chemical Name:C₃₅H₄₈Cl₂N₂O₃
CAS No.:1220903-14-9
Molecular Formula:C₃₅H₄₈Cl₂N₂O₃
Molecular Weight:615.684
Hs Code.:

C<sub>35</sub>H<sub>48</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₃₅H₄₈Cl₂N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₄₈Cl₂N₂O₃

Chemical Property:

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Technology Process of C₃₅H₄₈Cl₂N₂O₃

There total 8 articles about C₃₅H₄₈Cl₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1220903-13-8
isopropyl 4-((1R)-1-(2-amino-2-(3,5-dichlorophenyl)acetamido)-4,4-dimethylpentyl)benzoate

: 98-53-3
4-tercbutyl-cyclohexanone

: 1220903-14-9
C₃₅H₄₈Cl₂N₂O₃

Guidance literature:: With triethylamine; In isopropyl alcohol; at 130 ℃; for 5h; Microwave irradiation; Molecular sieve;

Reference yield:

: 70240-29-8
4-(isopropyloxycarbonyl)benzaldehyde

: 1220903-14-9
C₃₅H₄₈Cl₂N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate / dichloromethane / 30 h / 42 °C

2.1: iodine; magnesium / diethyl ether / 2.75 h / Reflux; Inert atmosphere

2.2: 2 h / -78 - 20 °C

2.3: 0 °C

3.1: hydrogenchloride; methanol / 1,4-dioxane / 1.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / acetonitrile / 18 h / 25 °C

5.1: trifluoroacetic acid / dichloromethane / 18 h / 25 °C

6.1: triethylamine / isopropyl alcohol / 5 h / 130 °C / Microwave irradiation; Molecular sieve

With hydrogenchloride; methanol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; iodine; caesium carbonate; magnesium; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,4-dioxane; diethyl ether; dichloromethane; isopropyl alcohol; acetonitrile;

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1220903-14-9
C₃₅H₄₈Cl₂N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide; tetrahydrofuran / 64 h / 70 °C

2.1: caesium carbonate / dichloromethane / 30 h / 42 °C

3.1: iodine; magnesium / diethyl ether / 2.75 h / Reflux; Inert atmosphere

3.2: 2 h / -78 - 20 °C

3.3: 0 °C

4.1: hydrogenchloride; methanol / 1,4-dioxane / 1.5 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / acetonitrile / 18 h / 25 °C

6.1: trifluoroacetic acid / dichloromethane / 18 h / 25 °C

7.1: triethylamine / isopropyl alcohol / 5 h / 130 °C / Microwave irradiation; Molecular sieve

With hydrogenchloride; methanol; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; iodine; potassium carbonate; caesium carbonate; magnesium; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;