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C5H5FeC5H4C6H4NCH3COC6H3(OCH3)2

Base Information
  • Chemical Name:C5H5FeC5H4C6H4NCH3COC6H3(OCH3)2
  • CAS No.:442873-85-0
  • Molecular Formula:C26H25FeNO3
  • Molecular Weight:455.336
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>FeC<sub>5</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>NCH<sub>3</sub>COC<sub>6</sub>H<sub>3</sub>(OCH<sub>3</sub>)2

Synonyms:C5H5FeC5H4C6H4NCH3COC6H3(OCH3)2

Suppliers and Price of C5H5FeC5H4C6H4NCH3COC6H3(OCH3)2
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Chemical Property of C5H5FeC5H4C6H4NCH3COC6H3(OCH3)2
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Technology Process of C5H5FeC5H4C6H4NCH3COC6H3(OCH3)2

There total 1 articles about C5H5FeC5H4C6H4NCH3COC6H3(OCH3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With Maleic hydrazide; In tetrahydrofuran; a soln. of complex in THF was treated with CH3I adn NaH at room temp. under N2, the mixt. was stirred at room temp. for 10 min then warmed at 60°C under N2 at 1.5 h, then at room temp. for 2 h; the solvent was removed, recrystd. from ethanol;
DOI:10.1021/ja026441v
Guidance literature:
With boron tribromide; lead dioxide; In dichloromethane; a soln. of complex and PbO2 in CH2Cl2 was stirred at 78°C for 1 hunder O2, a soln. of BBr3 in CH2Cl2 was added dropwise at -78°C, stirred at -78°C for 10 min then at room temp. overnight; H2O and satd. NaHCO3 was added, the organic phase was dried over Na2SO4,filtered, the solvent was removed, recrystd. from CHCl3 and hexane;
DOI:10.1021/ja026441v
upstream raw materials:

(C5H5)Fe(C5H4C6H4NHCOC6H3(OCH3)2)

methyl iodide

Downstream raw materials:

C5H5FeC5H4C6H4NCH3COC6H3O2

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