N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane

Base Information

Chemical Name:N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane
CAS No.:137945-95-0
Molecular Formula:C₂₄H₃₁N₃O₅
Molecular Weight:441.527
Hs Code.:

N<sup>1</sup>-(carbobenzyloxy)-N<sup>4</sup>-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane

Synonyms:N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane

Suppliers and Price of N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane

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Technology Process of N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane

There total 1 articles about N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 51440-81-4
3-benzyloxycarbonylaminobutyric acid

: 18807-73-3
N-benzyloxycarbonyl-1,4-butanediamine hydrochloride

: 137945-95-0
N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 36h;
DOI:10.1021/jm00082a013

Reference yield:

: 137945-95-0
N¹-(carbobenzyloxy)-N⁴-<3-<(carbobenzyloxy)amino>butyryl>-1,4-diaminobutane

: 137946-02-2
1,8-diamino-5-azanonane

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / methanol / 24 h / 2068.6 Torr

2: BH₃*THF / tetrahydrofuran / 1.) reflux, 48 h, 2.) RT, 24 h

With borane-THF; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm00082a013