5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate

Base Information

Chemical Name:5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate
CAS No.:1403889-63-3
Molecular Formula:C₁₉H₂₅NO₆S₂
Molecular Weight:427.543
Hs Code.:

Synonyms:5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate

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Chemical Property of 5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate

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Technology Process of 5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate

There total 5 articles about 5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 591-87-7
Allyl acetate

: 1403889-59-7
S-2-(acetoxy(p-tolyl)amino)-2-oxoethyl O-ethyl carbonodithioate

: 1403889-63-3
5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate

Guidance literature:: With dilauryl peroxide; In ethyl acetate; for 3h; Reflux; Inert atmosphere;
DOI:10.1021/ol3026044

Reference yield:

: 623-10-9
N-(4-methylphenyl)hydroxylamine

: 1403889-63-3
5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / diethyl ether; water / -5 °C / Cooling with ice; Inert atmosphere

2: acetic anhydride / 20 °C / Inert atmosphere

3: acetone / 6 h / 0 °C / Inert atmosphere

4: dilauryl peroxide / ethyl acetate / 3 h / Reflux; Inert atmosphere

With dilauryl peroxide; acetic anhydride; sodium hydrogencarbonate; In diethyl ether; water; ethyl acetate; acetone;
DOI:10.1021/ol3026044

Reference yield:

: 1403889-48-4
N-(4-methylphenyl)-2-chloro-N-hydroxyacetamide

: 1403889-63-3
5-(acetoxy(p-tolyl)amino)-2-(ethoxycarbonothioylthio)-5-oxopentyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / 20 °C / Inert atmosphere

2: acetone / 6 h / 0 °C / Inert atmosphere

3: dilauryl peroxide / ethyl acetate / 3 h / Reflux; Inert atmosphere

With dilauryl peroxide; acetic anhydride; In ethyl acetate; acetone;
DOI:10.1021/ol3026044