2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester

Base Information

Chemical Name:2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester
CAS No.:302576-70-1
Molecular Formula:C₃₀H₄₃NO₄SSi₂
Molecular Weight:569.913
Hs Code.:

Synonyms:2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester

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Chemical Property of 2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester

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Technology Process of 2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester

There total 3 articles about 2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 302576-68-7
2-(4-((phenoxythioxomethyl)amino)phenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester

: 302576-70-1
2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester

Guidance literature:: With trichlorosilane; triethylamine; In benzene; at 20 ℃; for 1h;
DOI:10.1016/S0968-0896(01)00075-X

Reference yield:

: 302576-99-4
2-(4-((phenoxythioxomethyl)amino)phenyl)methan-1-ol

: 302576-70-1
2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / pyridine / toluene / 20 °C

2: 98 percent / Et₃N; HSiCl₃ / benzene / 1 h / 20 °C

With pyridine; trichlorosilane; triethylamine; In toluene; benzene;
DOI:10.1016/S0968-0896(01)00075-X

Reference yield:

: 104-10-9
2-(4'-aminophenyl)ethyl alcohol

: 302576-70-1
2-(4-isothiocyanatophenyl)ethyl O,O-(3,4-bis(1,1,2,2-tetramethyl-1-silapropyl))caffeic acid ester

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / tetrahydrofuran / 0.5 h / 20 °C

2: 48 percent / pyridine / toluene / 20 °C

3: 98 percent / Et₃N; HSiCl₃ / benzene / 1 h / 20 °C

With pyridine; trichlorosilane; triethylamine; In tetrahydrofuran; toluene; benzene;
DOI:10.1016/S0968-0896(01)00075-X