ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate

Base Information

Chemical Name:ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate
CAS No.:1190854-47-7
Molecular Formula:C₁₈H₂₂N₂O₆S₂
Molecular Weight:426.514
Hs Code.:

Synonyms:ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate

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Chemical Property of ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate

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Technology Process of ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate

There total 1 articles about ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1190854-45-5
1-[2,6-dimethoxy-4-(methoxymethyl)phenyl]ethanone

: 26648-11-3
potassium hydrazine carbodithioate

: 36239-09-5
ethyl chlorocarbonylacetate

: 1190854-47-7
ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate

Guidance literature:: 1-[2,6-dimethoxy-4-(methoxymethyl)phenyl]ethanone; With t-butyldimethylsiyl triflate; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;

With N-Bromosuccinimide; In tetrahydrofuran; at 0 ℃; for 1.5h;

potassium hydrazine carbodithioate; ethyl chlorocarbonylacetate;

Reference yield:

: 1190854-47-7
ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate

: 1190854-49-9
ethyl 3-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-6-hydroxypyrazolo[5,1-b][1,3]thiazole-7-carboxylate

Guidance literature:: ethyl 3-{[4-(2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-thioxo-1,3-thiazole-3(2H)-yl]-amino}-3-oxopropanoate; With methyl iodide; In acetone; at 10 - 35 ℃; for 23h;

With potassium tert-butylate; In tert-butyl alcohol; at 10 - 35 ℃; for 3.5h;

With hydrogenchloride; In water; tert-butyl alcohol; pH=4; Cooling;