(-)-2-methyl-3-oxopropyl benzoate

Base Information

Chemical Name:(-)-2-methyl-3-oxopropyl benzoate
CAS No.:1076231-00-9
Molecular Formula:C₁₁H₁₂O₃
Molecular Weight:192.214
Hs Code.:

Synonyms:(-)-2-methyl-3-oxopropyl benzoate

Suppliers and Price of (-)-2-methyl-3-oxopropyl benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (-)-2-methyl-3-oxopropyl benzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (-)-2-methyl-3-oxopropyl benzoate

There total 1 articles about (-)-2-methyl-3-oxopropyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 141978-58-7
(S)-3-hydroxy-2-methylpropyl benzoate

: 1076231-00-9
(-)-2-methyl-3-oxopropyl benzoate

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/chem.200800623

Reference yield:

: 590-18-1
(Z)-2-Butene

: 1076231-00-9
(-)-2-methyl-3-oxopropyl benzoate

: C₁₆H₂₂O₂

Guidance literature:: (Z)-2-Butene; With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; n-heptane; at -45 ℃;

With (+)-β-methoxydiisopinocampheylborane; In tetrahydrofuran; at -78 ℃; for 1h;

(-)-2-methyl-3-oxopropyl benzoate; Further stages;
DOI:10.1002/chem.201502861

Reference yield:

: 627-40-7
methylallylether

: 1076231-00-9
(-)-2-methyl-3-oxopropyl benzoate

: 99438-28-5
(+)-B-methoxydiisocamphenylborane

: (2R,3S,4S)-3-hydroxy-4-methoxy-2-methylhex-5-en-1-yl benzoate

: (2S,3S,4S)-3-hydroxy-4-methoxy-2-methylhex-5-en-1-yl benzoate

Guidance literature:: methylallylether; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃;

(+)-B-methoxydiisocamphenylborane; In tetrahydrofuran; cyclohexane;

(-)-2-methyl-3-oxopropyl benzoate; Overall yield = 75 %; Overall yield = 1.12 g; Further stages;
DOI:10.1002/ejoc.201600988