N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide

Base Information

• Chemical Name: N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide
• CAS No.: 127349-06-8
• Molecular Formula: C₂₂H₂₂N₂O₄S
• Molecular Weight: 410.494
• Mol file: 127349-06-8.mol

Synonyms:N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide

Chemical Property of N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide

There total 2 articles about N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

bis(p-methoxyphenyl)methanone (90-96-0) + toluene-4-sulfonic acid hydrazide (1576-35-8) → N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide (127349-06-8)

Guidance literature:

With acetyl chloride; In ethanol; for 40h; Heating;

DOI:10.1021/ol0711117

Reference yield:

→ N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide (127349-06-8)

Guidance literature:

/BRN= 3360625/;

Reference yield: 63.0%

benzyl diethyl phosphate (884-90-2) + N′-(bis(4-methoxyphenyl)-methylene)-4-methylbenzenesulfonohydrazide (127349-06-8) → 1,1-bis(4-methoxyphenyl)-2-phenylethene (26642-57-9)

Guidance literature:

With dichloro bis(acetonitrile) palladium(II); 1,3-bis-(diphenylphosphino)propane; lithium tert-butoxide; at 70 ℃; for 3h; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.joc.1c02580

upstream raw materials:

bis(p-methoxyphenyl)methanone

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

1,1,2,2-tetrakis(4-methoxyphenyl)ethene

bis(4-methoxyphenyl)methano<60>fullerene

2-(bis(4-methoxyphenyl)methyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

4,4’-(propa-1,2-diene-1,1-diyl)bis(methoxybenzene)