methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Base Information

Chemical Name:methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate
CAS No.:1356600-41-3
Molecular Formula:C₃₁H₃₂N₂O₆
Molecular Weight:528.605
Hs Code.:

Synonyms:methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

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Chemical Property of methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

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Technology Process of methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

There total 7 articles about methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1356600-26-4
2-(4-(bromomethyl)phenoxy)-1-phenylethanone O-methyl oxime

: 1356600-40-2
methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-(4-hydroxyphenyl)propanoate

: 1356600-41-3
methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: With potassium carbonate; In acetonitrile; at 0 - 65 ℃; for 14h;

Reference yield:

: 7400-08-0,50940-26-6
p-Coumaric Acid

: 1356600-41-3
methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / 16 h / 130 °C / Neat (no solvent); Sealed tube

2: methanesulfonic acid / 1 h / 6 °C

3: potassium carbonate / acetonitrile / 14 h / 0 - 65 °C

With aluminum (III) chloride; methanesulfonic acid; potassium carbonate; In acetonitrile;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1356600-41-3
methyl 3-(3,5-dimethyl-1,2-oxazol-4-yl)-3-{4-[(4-{[(2E,2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate; acetic acid / 0.08 h / 20 °C

1.2: 3 h / 20 - 80 °C

2.1: potassium carbonate / acetonitrile / 0.08 h / 20 °C

2.2: 5 h / 20 - 80 °C

3.1: phosphorus tribromide / dichloromethane / 0.5 h / 0 - 20 °C

4.1: potassium carbonate / acetonitrile / 14 h / 0 - 65 °C

With sodium acetate; phosphorus tribromide; potassium carbonate; acetic acid; In dichloromethane; acetonitrile;