(2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine

Base Information

Chemical Name:(2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine
CAS No.:132065-47-5
Molecular Formula:C₂₃H₂₉NO₃SSe
Molecular Weight:478.514
Hs Code.:

Synonyms:(2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine

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Chemical Property of (2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine

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Technology Process of (2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine

There total 7 articles about (2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 71338-47-1
2-phenylselenoacetaldehyde diethylacetal

: 132065-46-4,132065-52-2
(3RS,4S)-6-methyl-4-(p-tolylsulfonylamino)hept-1-en-3-ol

: 132065-47-5
(2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine

Guidance literature:: With pyridinium p-toluenesulfonate; In toluene; for 2h; Heating;
DOI:10.1016/0957-4166(90)80009-N

Reference yield:

: 117248-23-4,132065-38-4
(3RS,4S)-4-amino-6-methylhept-1-en-3-ol

: 132065-47-5
(2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Et₃N / tetrahydrofuran; H₂O / 1.) 0 deg C, 30 min, 2.) room temperature, overnight

2: 97 percent / PPTS / toluene / 1 h / Heating

With pyridinium p-toluenesulfonate; triethylamine; In tetrahydrofuran; water; toluene;

Reference yield:

: 107599-94-0,107600-11-3,112190-40-6
3-hydroxy-6-methyl-4(S)-<(triphenylmethyl)amino>-1-heptene

: 132065-47-5
(2RS,4S,5RS)-4-isobutyl-2-phenylselenanylmethyl-3-(p-tolylsulfonyl)-5-vinyloxazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / DOWEX-50-X₈ / methanol / 16 h / Ambient temperature

2: 81 percent / Et₃N / tetrahydrofuran; H₂O / 1.) 0 deg C, 30 min, 2.) room temperature, overnight

3: 97 percent / PPTS / toluene / 1 h / Heating

With DOWEX-50-X₈; pyridinium p-toluenesulfonate; triethylamine; In tetrahydrofuran; methanol; water; toluene;