4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester

Base Information

Chemical Name:4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester
CAS No.:131911-53-0
Molecular Formula:C₃₀H₃₃F₂NO₄
Molecular Weight:509.593
Hs Code.:

4-<3-<4-<bis(4-fluorophenyl)methyl>-1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester

Synonyms:4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester

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Chemical Property of 4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester

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Technology Process of 4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester

There total 5 articles about 4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.9%

: 131911-53-0
4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester

Guidance literature:

Reference yield:

: 60285-00-9
4-[bis(4-fluorophenyl)-methyl]piperidine

: 131911-53-0
4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃ / butan-1-ol / 21 h / Heating

2: SOCl₂ / CHCl₃ / 6 h / Heating

3: 1.) NaH / 1.) DMSO, RT, 0.5 h, 2.) DMSO, 60 deg C, overnight

With thionyl chloride; sodium hydride; sodium hydrogencarbonate; In chloroform; butan-1-ol;
DOI:10.1021/jm00114a009

Reference yield:

: 58113-36-3
4-(bis(4-fluorophenyl)methylene)piperidine

: 131911-53-0
4-<3-<4--1-piperidinyl>propoxy>-3-methoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: I₂, phosphorous, methanesulfonic acid / aq. acetic acid / 7 h / Heating

2: NaHCO₃ / butan-1-ol / 21 h / Heating

3: SOCl₂ / CHCl₃ / 6 h / Heating

4: 1.) NaH / 1.) DMSO, RT, 0.5 h, 2.) DMSO, 60 deg C, overnight

With phosphorus; thionyl chloride; methanesulfonic acid; iodine; sodium hydride; sodium hydrogencarbonate; In chloroform; acetic acid; butan-1-ol;
DOI:10.1021/jm00114a009