C₅₆H₆₁N₈O₉P

Base Information

Chemical Name:C₅₆H₆₁N₈O₉P
CAS No.:1367204-59-8
Molecular Formula:C₅₆H₆₁N₈O₉P
Molecular Weight:1021.12
Hs Code.:

C<sub>56</sub>H<sub>61</sub>N<sub>8</sub>O<sub>9</sub>P

Synonyms:C₅₆H₆₁N₈O₉P

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Chemical Property of C₅₆H₆₁N₈O₉P

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Technology Process of C₅₆H₆₁N₈O₉P

There total 7 articles about C₅₆H₆₁N₈O₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1367204-50-9
C₄₇H₄₄N₆O₈

: 102691-36-1
N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

: 1367204-59-8
C₅₆H₆₁N₈O₉P

Guidance literature:: With DCI; In dichloromethane; acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/cbic.201100573

Reference yield:

: 211676-15-2
8-bromo-3′,5′-O-bis(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 1367204-59-8
C₅₆H₆₁N₈O₉P

Guidance literature:: Multi-step reaction with 6 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 95 °C

2: pyridine / 20 °C / Inert atmosphere

3: pyridine; dmap / 20 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 48 h / 20 °C

5: pyridine; silver nitrate / 3 h / 20 °C / Inert atmosphere

6: DCI / dichloromethane; acetonitrile / 2 h / 20 °C / Inert atmosphere

With pyridine; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrabutyl ammonium fluoride; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; silver nitrate; acetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; acetonitrile; 1: Buchwald-Hartwig cross-coupling;
DOI:10.1002/cbic.201100573

Reference yield:

: 1367204-28-1
C₃₈H₅₄N₆O₆Si₂

: 1367204-59-8
C₅₆H₆₁N₈O₉P

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 48 h / 20 °C

2: pyridine; silver nitrate / 3 h / 20 °C / Inert atmosphere

3: DCI / dichloromethane; acetonitrile / 2 h / 20 °C / Inert atmosphere

With pyridine; tetrabutyl ammonium fluoride; silver nitrate; acetic acid; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/cbic.201100573