6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside

Base Information

Chemical Name:6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside
CAS No.:111829-03-9
Molecular Formula:C₆₉H₆₂O₁₀
Molecular Weight:1051.25
Hs Code.:

Synonyms:6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside

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Chemical Property of 6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside

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Technology Process of 6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside

There total 4 articles about 6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 35674-14-7
1,6-di-O-trityl-β-D-fructofuranosyl 6-O-trityl-α-D-glucopyranoside

: 111829-03-9
6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; for 0.25h; Ambient temperature;
DOI:10.1016/0008-6215(87)80215-X

Reference yield:

: 67909-34-6
3,6'-di-O-acetyl-4,6:2,1'-di-O-isopropylidene-tagato-sucrose

: 111829-03-9
6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / diethyl azodicarboxylate, triphenylphosphine / toluene / 0.5 h / Ambient temperature

2: 90 percent / aqueous 60percent acetic acid / 0.17 h / 80 °C

3: 89 percent / sodium methoxide / methanol

4: 56.3 percent / pyridine / 6 h / 70 °C

With sodium methylate; acetic acid; triphenylphosphine; diethylazodicarboxylate; In pyridine; methanol; toluene;
DOI:10.1016/0008-6215(87)80215-X

Reference yield:

: 67909-41-5,67909-42-6,104012-35-3
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl 1,6,-di-O-acetyl-3,4-anhydro-β-D-lyxo-hexulofuranoside

: 111829-03-9
6-O-trityl-α-D-glucopyranosyl 3,4-anhydro-1,6-di-O-trityl-β-D-lyxo-hexulofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / sodium methoxide / methanol

2: 56.3 percent / pyridine / 6 h / 70 °C

With sodium methylate; In pyridine; methanol;
DOI:10.1016/0008-6215(87)80215-X