trans-2-cyclopropanemethanol

Base Information

Chemical Name:trans-2-cyclopropanemethanol
CAS No.:114095-63-5
Molecular Formula:C₁₁H₁₁F₃O
Molecular Weight:216.203
Hs Code.:

trans-2-<m-(trifluoromethyl)phenyl>cyclopropanemethanol

Synonyms:trans-2-cyclopropanemethanol

Suppliers and Price of trans-2-cyclopropanemethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-2-cyclopropanemethanol

Chemical Property:

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Technology Process of trans-2-cyclopropanemethanol

There total 5 articles about trans-2-cyclopropanemethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 243665-18-1
trans-2-(3-(trifluoromethyl)phenyl)cyclopropanecarboxylic acid

: 114095-63-5
trans-2-cyclopropanemethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1139/cjc-77-5-6-1123

Reference yield:

: 1977-59-9,114095-57-7
ethyl trans-2-cyclopropane-1-carboxylate

: 114095-63-5
trans-2-cyclopropanemethanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 6h; Heating;
DOI:10.1021/ja00219a040

Reference yield:

: 454-89-7
3-Trifluoromethylbenzaldehyde

: 114095-63-5
trans-2-cyclopropanemethanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 99 percent / CH₂Cl₂ / 16 h / 20 °C

2.1: NaH / dimethylsulfoxide / 1 h / 20 °C

2.2: 87 percent / dimethylsulfoxide / 6 h

3.1: 95 percent / aq. potassium tert-butoxide / diethyl ether / 16 h / 20 °C

4.1: 87 percent / LiAlH₄ / tetrahydrofuran / 2 h / 0 °C

With lithium aluminium tetrahydride; potassium tert-butylate; sodium hydride; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; 1.1: Condensation / 2.1: Metallation / 2.2: cyclopropanation / 3.1: Hydrolysis / 4.1: Reduction;
DOI:10.1139/cjc-77-5-6-1123