1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

Base Information

Chemical Name:1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate
CAS No.:1346576-24-6
Molecular Formula:C₁₉H₂₄N₂O₃
Molecular Weight:328.411
Hs Code.:

Synonyms:1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

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Chemical Property of 1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

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Technology Process of 1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

There total 4 articles about 1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 3318-61-4
1-phenyl-2,4-pentanedione

: 107-91-5
cyanoacetic acid amide

: 1346576-24-6
1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

: 1346576-23-5
1,1-dimethylethyl {[4-methyl-2-oxo-6-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

Guidance literature:: 1-phenyl-2,4-pentanedione; cyanoacetic acid amide; With piperidine; In ethanol; at 75 ℃; Reflux;

With sodium acetate; acetic acid; platinum(IV) oxide; palladium 10% on activated carbon; for 12h; under 2327.23 Torr; Inert atmosphere; Sealed vessel;

di-tert-butyl dicarbonate; With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h;

Reference yield:

: 1346576-21-3
3-(aminomethyl)-6-methyl-4-(phenylmethyl)-2(1H)-pyridinone

: 1346576-22-4
3-(aminomethyl)-4-methyl-6-(phenylmethyl)-2(1H)-pyridinone

: 1346576-24-6
1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

: 1346576-23-5
1,1-dimethylethyl {[4-methyl-2-oxo-6-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

Guidance literature:: With di-tert-butyl dicarbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h;

Reference yield:

: 101-97-3
Ethyl 2-phenylethanoate

: 1346576-24-6
1,1-dimethylethyl {[6-methyl-2-oxo-4-(phenylmethyl)-1,2-dihydro-3-pyridinyl]methyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium amide / diethyl ether / -5 - 20 °C / Reflux; Inert atmosphere

1.2: pH 4 - 5

2.1: piperidine / ethanol / 75 °C / Reflux

2.2: 12 h / 2327.23 Torr / Inert atmosphere; Sealed vessel

2.3: 4 h / 0 - 20 °C

With piperidine; sodium amide; In diethyl ether; ethanol;